Hot Isostatic Pressing Technology for Indian Test Blanket Module Fabrication
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Hot Isostatic Pressing Technology for Indian Test Blanket Module Fabrication. Dr. G. Appa Rao. Defence Metallurgical Research Laboratory Kanchanbagh PO, Hyderabad-500058, India. Email: [email protected] 22 July 2008. Introduction.

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Hot isostatic pressing technology for indian test blanket module fabrication

Hot Isostatic Pressing Technology for Indian Test Blanket Module Fabrication

Dr. G. Appa Rao

Defence Metallurgical Research Laboratory

Kanchanbagh PO, Hyderabad-500058, India.

Email: [email protected]

22 July 2008.


Hot isostatic pressing technology for indian test blanket module fabrication

Introduction

  • Selection of appropriate materials and fabrication technologies for various components for fusion reactors relies on trade-off between multiple requirements which are mainly driven by:

    • Economic

    • Safety and

    • Environmental effects

  • Materials:

    • Martensitic steels

    • Non-Ferrous alloys

    • Ceramics

    • Vanadium alloys

    • SiC/SiC Composites

    • Ti and Cr alloys

  • Fabrication Technologies:

    • Cutting and machining

    • Special welding techniques

    • Investment casting

    • Hot isostatic pressing (HIP)


Hot isostatic pressing technology for indian test blanket module fabrication

Significance of HIP Technology

  • Implementation and joining of F/M steels are an important

  • goal due to the complex geometry of the blanket modules.

  • Necessity for reducing the leak level and maintenance.

  • Advanced techniques based on solid or powder HIP are to

  • be established


Hot isostatic pressing technology for indian test blanket module fabrication

Principles of Isostatic Pressing

Pascal’s Law


Hot isostatic pressing technology for indian test blanket module fabrication

Isostatic Pressing

Cold Isostatic Pressing

(CIP) 1913

Warm Isostatic Pressing

(WIP) 1960

Hot Isostatic Pressing

(HIP) 1955

~300 ºC

2000 ºC

Temp.

RT.

Inert gas

Pressure

medium

Water +oil

Water +oil

200 MPa

200 MPa

Pressure

400 MPa

Steel,

Ceramic & Glass

Powder

container

Rubber

Rubber

Full density

Full density

Green compaction

Extent of

densification


Hot isostatic pressing technology for indian test blanket module fabrication

Hot Isostatic Pressing

  • HIP is a an innovative thermal treatment process subjects the

  • material / component to a combination of high pressure and

  • elevated temperature

  • HIP results in near theoretical density, uniform microstructure

  • and consistent mechanical properties

HIPing Parameters:

Temperature : 0.7 - 0.9 Tm

Pressure : 100-200 MPa

Time : 2- 4 h.


Hot isostatic pressing technology for indian test blanket module fabrication

Details of HIP Equipment


Hot isostatic pressing technology for indian test blanket module fabrication

Densification Mechanisms of HIPing

  • Particle rearrangement

  • Plasticity

  • Power-law creep and

  • Volume and grain boundary diffusion


Hot isostatic pressing technology for indian test blanket module fabrication

Stages of HIP Densification


Hot isostatic pressing technology for indian test blanket module fabrication

HIP Diagrams


Hot isostatic pressing technology for indian test blanket module fabrication

Applications of HIP Technology

  • Cladding

  • Diffusion Bonding

  • Consolidation of Encapsulated Powder

  • Densification of Metal castings

  • Specialized Applications:

  • Medical Implants

  • HIP of ultra fine Tungsten Carbide Cobalt Hard Metals

  • Rejuvenation of Deteriorated Components

  • Formation and Control of Pores

  • Joining of Fusion Reactor Components


Hot isostatic pressing technology for indian test blanket module fabrication

100

AS-HIP

75

HIP

+

H .W

Cost Reduction Potential, %

50

25

Conventional

Processing

0

Cost Reduction Potential for a

Selected Group of Superalloy Parts


Hot isostatic pressing technology for indian test blanket module fabrication

CIP and HIP Facilities at DMRL

(200 Dia. X 600 HT.) mm

400 MPa

(100 Dia. X 200 HT.) mm, 200 MPa

1450, 2000 ºC

(650 Dia. X 1200 HT.) mm, 200 MPa

1450ºC

(270 Dia. X 990 HT.) mm, 200 MPa

1450ºC


Hot isostatic pressing technology for indian test blanket module fabrication

40 mm

Spec.

As-HIPed

HIPing of Stainless Steel Powder

G. Appa Rao and M.Kumar, Mater.Sci. and Technol. 1997


Hot isostatic pressing technology for indian test blanket module fabrication

Stainless Steel Integral Turbine Rotor

Superalloy 718 Integral Turbine Rotor

Potential of HIP for Complex Shapes


Hot isostatic pressing technology for indian test blanket module fabrication

HIP Diffusion Bonding of Materials

  • Advantages:

  • Similar and dissimilar material can be joined

  • Complex shape can be joined easily

  • Original microstructure remains intact

  • ODS and FRM can be joined

  • Joint integrity is better than that of conventional one

  • Material forms for HIP bonding:

  • Powder-powder

  • Powder-solid

  • Solid -solid


Hot isostatic pressing technology for indian test blanket module fabrication

SS -Solid

Cu-Solid

Shaft alloy

Disk alloy

SS-Powder

Cu-Powder

Microstructure of HIP Diffusion Bonded Materials

G. Appa Rao et. al, DMRL TR2000265 (2000)


Hot isostatic pressing technology for indian test blanket module fabrication

Spec.

DMRL

DMRL

Spec.

Mechanical Properties of HIP Diffusion Bonded Alloys

Failure did not occur at the joint


Hot isostatic pressing technology for indian test blanket module fabrication

P/M(HIP) Diffusion Bonded Hardware (DMRL)

Prototype thrust chamber clouseout

Ni-base superalloy components


Hot isostatic pressing technology for indian test blanket module fabrication

Overview of Blanket Module Fabrication

(Literature)

  • Reduced Activation Ferritic Martensitic (RAFMA) steel is the

  • structural material for TBMs

  • Fabrication concepts rely on plates with internal cooling channels

Main technologies for fabrication of TBMs:

  • Cutting and machining of semi finished products

  • Joining of parts to produce the plates with internal channels

  • Bending of cooling plates

  • Heat treatment to improve the structure and properties


Hot isostatic pressing technology for indian test blanket module fabrication

Configuration Details of Blanket Module


Hot isostatic pressing technology for indian test blanket module fabrication

First Wall Fabrication Procedures

(a) Two-Step HIPing Method:

  • Involves machined grooved plates

  • Use of Mo- alloy massive stiffening / supporting plates between

  • the encapsulation and the FW/CP plates

  • HIPing at low pressure to achieve bonding at the Interface

  • Removal of encapsulation and Mo plates and drilling of channels

  • The FW is further HIPed at high pressure to achieve full bonding

  • Heat treatment, testing and evaluation


Hot isostatic pressing technology for indian test blanket module fabrication

(b) Single High Pressure HIPing Method / HIP forming Process:

  • Involves insertion of round tubes in the rectangular grooves

  • Ends of the tubes are welded to the plates but the tubes are not closed

  • During HIPing, the tubes expand and conform to the grooves

  • Mo- alloy supporting plates are not required

  • Heat treatment, testing and evaluation.


Hot isostatic pressing technology for indian test blanket module fabrication

(c) Rectangular Tube (RT) Process:

  • Involves diffusion welding of RTs. and cover plates

  • HIPing to improve the joint integrity

  • No need for stiffening plates

  • There is a scope for bending the RTs. and cover plates before HIPing.

  • Heat treatment, testing and evaluation


Hot isostatic pressing technology for indian test blanket module fabrication

FW mock up manufactured by HIP forming ( top: parts before HIP;

bottom: mock up after HIP, bending and marching.


Hot isostatic pressing technology for indian test blanket module fabrication

Conclusions

  • Fabrication of test blanket modules (TBMs) is a technologically

  • challenging task

  • Hot isostatic pressing (HIP) is a promising technology for

  • fabrication of TBMs

  • Considerable expertise on several aspects of HIP technology is

  • available at DMRL to address various issues in this

  • field

  • Study on development of prototype TBM components can be

  • taken up with the existing infrastructure.


Hot isostatic pressing technology for indian test blanket module fabrication

Thank you


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