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Long term annealing of neutron irradiated detectors evaluated at LHC operational temperatures

Long term annealing of neutron irradiated detectors evaluated at LHC operational temperatures. E. Verbitskaya , V. Eremin, I. Ilyashenko Ioffe Physico-Technical Institute of Russian Academy of Sciences St. Petersburg, Russia Z. Li Brookhaven National Laboratory, Upton, NY, USA J. Härkönen

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Long term annealing of neutron irradiated detectors evaluated at LHC operational temperatures

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  1. Long term annealing of neutron irradiated detectors evaluated at LHC operational temperatures E. Verbitskaya, V. Eremin, I. Ilyashenko Ioffe Physico-Technical Institute of Russian Academy of Sciences St. Petersburg, Russia Z. Li Brookhaven National Laboratory, Upton, NY, USA J. Härkönen Helsinki Institute of Physics, CERN/PH, Geneva, Switzerland Marko Mikuž, Vladimir Cindro Jožef Stefan Institute, Ljubljana Chris Parkes Glasgow University 8 RD50 Collaboration Workshop Prague, June 25-28, 2006

  2. Type of Si Processing Radiation characteristics of heavily irradiated detectors Technotest Goal of the project: Finding correlations and comparison of radiation hardness with respect to: E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  3. Technotest Participants Detector processing: ♦Ioffe Physico-Technical Institute (PTI) + Research Institute of Material Science and Technology (RIMST) ♦ BNL ♦ Helsinki Institute of Physics (HIP) Irradiation: ♦ CERN (protons 24 GeV/c) ♦ Iosef Stefan Institute, Ljubljana (neutrons 1 MeV) Evaluation ♦ Ioffe Physico-Technical Institute ♦ BNL ♦ HIP ♦ Iosef Stefan Institute ♦ Glasgow University E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  4. Status of the work • Experiments carried out: •  detectors processed at three institutions  irradiated by 1 MeV neutrons, Fn = 11010- 51015 cm-2  irradiated by 24 GeV/c protons, Fp = 11014 and 11015 cm-2 1 MeV neutrons: pres. 5 RD50 Workshop, Florence I-V characteristics, TCT signal 24 GeV protons: pres. 7 RD50 Workshop, CERN SCSI in detectors from MCZ Si; Vfd and Neffinin long term annealing Current study in 2006 1 MeV neutrons: studies of annealing (initial stage)  detectors processed from MCZ and FZ n-type Si  annealing at 80°C E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  5. Experimental samples Resistivity, kW·cm n-Si FZ: 4-6 n-Si MCZ: 1 E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  6. Manufacturing procedure E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  7. Experimental annealings: 80C, steps with variable time  TCT using 840 nm laser pulse generation of free carriers, p+ side, n+ side Current pulse response is measured at RT and -15C (ATLAS) All measurements: range of bias voltage 20/50-900 V E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  8. Current pulse response, n-Si, Fn = 51013 cm-2 Before annealing PTI-Cz-c12, n+ side PTI-FZn2-b11, p+ side Before annealing: FZ Si: SCSI (-SC) MCZ Si : no SCSI (all samples) - evaluation of response from n+ side, hole collection V: 10-900 V E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  9. MCZ Si, Fn = 51013 cm-2:different processing RT RT -15 C RT tcoll is smaller at -15C E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  10. Fn = 5 e13 cm-2, tann= 76 min RT RT RT -15C E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  11. Evolution of response under annealing,MCZ Si, Fn = 51013 cm-2, V = 200 V, hole collection RT: detector is fully depleted, +Neff decreases – E becomes more uniform E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  12. Evolution of response under annealing 200 V Dependence of vdr vs. E and T Pulse width: depends on vdr(T) Difference: Low E: e – 30%, h – 50% High E: e, h – 10% E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  13. Q vs. V and tsh , MCZ n-Si, Fn = 51013 cm-2 tsh = 10 ns Total charge, RT tsh – shaping time E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  14. Q vs. V and tsh , MCZ n-Si, Fn = 51013 cm-2 E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  15. Current pulse response, MCZ n-Si, Fn = 51014 cm-2 Different processing p+ side, electron collection Before annealing V: 50-900 V RT RT Double Peak shape with different H1/H2 RT -15 C E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006 SCSI for all detectors, at RT and -15 C

  16. Fn = 5 e14 cm-2, tann= 156 min, RT H1/H2 ratio in DP is different: E(x) is different Practical aspect: tcoll is sensitive to technology E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  17. Fn = 5e14 cm-2, tann= 156 min, -15C At -15C: Pronounced DP with H1/H2>1 even at 900 V - reduction of E at n+ side E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  18. Evolution of response under annealingMCZ Si, Fn = 51014 cm-2 V = 500 V, RT Electron collection E(x) changes from full depletion to partial depletion at RT and -15C E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  19. Evolution of response under annealing,MCZ Si, Fn = 51014 cm-2, V = 500 V • is the same at RT and –15C • = 6 ns - lowest value! E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  20. Q vs. V under annealingMCZ n-Si, Fn = 51014 cm-2 Single peak  Double peak  E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  21. Q vs. V and tsh at RT and –15C Visible CCE reduction at tsh = 10 ns  Reduction is less at –15C(vdr) E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  22. Different processing, Q vs. V at RT Difference in H1/H2 E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  23. Vfd and Neff evaluated from pulse responseinitial annealing stage Vfd E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  24. Neff evaluated from pulse response Effective macroscopic parameters: As-irradiated MCZ Si detectors: Annealing 160 min: 5e13 cm-2: sensitive to processing reduces sensitivity 5e14 cm-2: no sensitivity E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  25. n+ p+ E2 E1 Eb Wb W2 W1 Reconstruction of E(x) from DP response Fn = 5e14 cm-2 p+ Electric field gradient dE/dx and Neff in the region adjacent to p+ contact are different and sensitive to detector processing  difference in balance of DDs and DAs induced by radiation E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  26. E(x) reconstruction HIP-Cz-66 PTI-Cz-d11 E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

  27. Conclusions Detectors from n-type MCZ silicon irradiated by 1MeV neutrons Fn = 51013 cm-2 • Space Charge (+) • Insignificant difference of pulse response before and after annealing  Fn = 51014 cm-2 • Space Charge (-) • DP current pulse shape dominates • H1/H2 is affected by technologyand changes under annealing • Annealing reduces difference in effective macroscopic parameters Protons, Fp = 11015 cm-2: influence of technology is still observed! RT  –15C: • trapping lifetime is the same • reduction of E at n+ side • higher drift velocity, reduction of current and dissipated power E. Verbitskaya et al., 8 RD50 Workshop, Prague, June 25-28, 2006

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