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Comprehensive Guide to Mercury Vapor Phase Analysis Methods

This guide details Method 30A and 30B for determining total mercury vapor phase, with specific requirements and waivers. It includes updates on Part 72 Permits Regulation and Part 75 Continuous Emission Monitoring procedures.

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Comprehensive Guide to Mercury Vapor Phase Analysis Methods

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  1. FR Optional Hg Methods Rulemaking 09/07/07: Method 30A • Method 30A begins page 51501 • Determines total vapor phase Hg • Full traversing req’d – unless (see 8.1.3) • Section 8.1.3 “Stratification” see 8.1.3.5 sub. SO2 until 01/01/09 (page 51504) • Section 8.2.7 “Dynamic Spiking” waived until 01/01/09 (page 51505) • QA/QC summary table page 51507

  2. FR Optional Hg Methods Rulemaking 09/07/07: Method 30B • Method 30B begins page 51518 • Intended for total vapor phase Hg • Traversing req’d – extent as per 30A • QA/QC summary table page 51522

  3. FR Optional Hg Methods Rulemaking 09/07/07: Other Included Items • Part 72 Permits Regulation - revision of sorbent trap monitoring system definition - page 51527 • Part 75 Continuous Emission Monitoring – various revisions and additions beginning on page 51527, including to Appendix K

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