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This study explores microcrack formation in cementitious materials and proposes detection methods using Gallium intrusion and crack examinations. By investigating autogenous shrinkage and crack development, the research aims to improve crack prevention strategies in high-performance concrete.
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Microcrack Detectionin High-Performance Cementitious Materials Pietro Lura, Ye Guang, Kyoji Tanaka, and Ole Mejlhede Jensen
Early-age cracking Tokyo Institute of Technology, Yokohama, Japan
Microcracking (Bisschop & van Mier 2002)
Chemical shrinkage Autogenous shrinkage Definitions (Jensen & Hansen 2001) solid water air
Autogenous shrinkage in HPC • Less water • More cement • Silica fume
Internal microcracking • Does autogenous shrinkage lead to internal cracks? • How to detect them?
Autogenous relative humidity Paste C (w/c 0.30 + 20% SF +0.6% SAP) Paste A (w/c 0.35) Paste B (w/c 0.30 + 20% SF)
Autogenous strain Paste C (w/c 0.30 + 20% SF +0.6% SAP) Paste A (w/c 0.35) Paste B (w/c 0.30 + 20% SF)
Samples for crack detection - 3 cement pastes • 1.5, 3, and 6-mm rods • sealed at 32C
10 1.2 µm ] 1 m µ [ r e t e m a i d e 0.1 r o P 0.01 1.6 MPa 0.1 1 10 100 Intrusion pressure [MPa] Properties of Gallium - melting point 29.8 C • does not wet cement paste • nontoxic
Sample preparation • epoxy resin • grinding • polishing • crack examination: - optical microscope - BSE - EPMA
Conclusions • Cracks before intrusion can be distinguished • High shrinkage, big rod Cracks
Further research • EPMA • Acoustic Emission • FE calculations