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APS8_34 - PowerPoint PPT Presentation


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APS8_34. Al90Tb10 RTO-2-9 MJK. Heated at 10C/min 6 s per scan Did a 21 point data smooth of T data T-t data file: APS8_34_heating_all_smooth21 Combined the 2 GE1 data sets as a first look Good data for c1_00311 Starts at 455s Crystallization begins at 1403 s Good data for c2_00312

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aps8 34

APS8_34

Al90Tb10RTO-2-9MJK

slide2

Heated at 10C/min

    • 6 s per scan
    • Did a 21 point data smooth of T data
      • T-t data file: APS8_34_heating_all_smooth21
  • Combined the 2 GE1 data sets as a first look
  • Good data for c1_00311
    • Starts at 455s
    • Crystallization begins at 1403 s
  • Good data for c2_00312
    • Starts at 1907 s
    • Cooling at 3251 s
time sequence
Time sequence
  • Initial crystallization
    • Initial ~ 229°C
    • Final ~ 237°C
  • 4 crystallization events
initial crystallization
Initial crystallization
  • Subtract scan 150
    • Small amount of fcc Al appears first
cry fraction only
Cry fraction only
  • Convert to two theta and then output in gsas format
  • Scan 1 is at time 1361, 220C