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AL CHEM REVIEW

ORGANIC CHEMISTRY. AL CHEM REVIEW. AL CHEM Written Practical [Organic Chemistry]. p.1. Distillation. Solvent Extraction (use separating funnel). Fractional Distillation. Common Separation Method. Physical Method. Chemical Method. Physical Method. p.2. Recrystallization.

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Experiment 14

Experiment 14. Preparation of Acetylsalicylic Acid. Objectives. Obtain experience in Organic Synthesis To isolate and purify your synthesized product Gain experience in organic chemistry techniques. Aspirin. The pharmaceutical ingredient in Aspirin tablets is acetylsalicylic acid

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Recrystallization

Q. 1 Why is the impure solid dissolved in the minimum quantity of hot solvent? If excess solvent is used, (a) some of the insoluble impurities shall remain in the filtrate in step 4. (b) the yield would drop as more solute will remain in the mother liquor in step 6.

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AL CHEM REVIEW

Experiment 14

Recrystallization