1 / 18

Chemical Analytical Center for Environmental Testing in Kazakhstan

Accredited testing laboratory for environmental samples including water, air, soil, and workplace assessments. Equipped with advanced instruments and staffed by highly skilled specialists trained in relevant standards.

ksarratt
Download Presentation

Chemical Analytical Center for Environmental Testing in Kazakhstan

An Image/Link below is provided (as is) to download presentation Download Policy: Content on the Website is provided to you AS IS for your information and personal use and may not be sold / licensed / shared on other websites without getting consent from its author. Content is provided to you AS IS for your information and personal use only. Download presentation by click this link. While downloading, if for some reason you are not able to download a presentation, the publisher may have deleted the file from their server. During download, if you can't get a presentation, the file might be deleted by the publisher.

E N D

Presentation Transcript

  1. KAZAKHSTAN AGENCY OF APPLIED ECOLOGY CHEMICAL-ANALYTICAL CENTER 2015

  2. CHEMICAL-ANALYTICAL CENTER Chemical-Analytical Center consists of: • Mobile Environmental Laboratory (MEL); • Testing Laboratory (Aktau). Testing Laboratory is accredited in accordance with the «ST RK ISO/IEC 17025-2007 - General requirements for competence of testing and calibration laboratories».

  3. SCOPE OF ACCREDITATION OF MEL Objects of analysis: • Sample collection: drinking water, natural water (surface and groundwater), wastewater (before and after treatment); • Sample collection: ground (soilsand bottom sediments); • Atmosphericairof residential and sanitary protection zones; • Air of operational areas; • Industrial emissions in the atmosphere; • Emissions from motor vehicles.

  4. Mobile EnvironmentalLaboratory Equipment • Gas analyzers GANK-4 (AP) produced by “SPA PRIBOR “GANK" (Russia) • Gas analyzer Testo-350 manufactured by "TestoAG" (Germany) • Gas analyzer Testo-350XLmanufactured by "TestoAG" (Germany) • Microclimate parameters measuring device "Meteoskop" produced by "NTM-Zaschita” (Russia) -6 units. • Electric and magnetic field parameters measuring device BE-meter AT-002, "NTM-Zaschita” (Russia) • Electrostatic field tension meter ST-01, "NTM-Zaschita” (Russia) • Luxmeter "TKA-Lux" STC“TKA” (Russia) • Bellows-sealed aspirators; single- andmulti-channel

  5. SCOPE OF ACCREDITATION OF TL Natural,drinking andwastewater: • Sample collection, totalmineralization, pH, fluoride, sulfates, chlorides, phosphates, nitrates, nitrites, ammoniumnitrogen, COD, BOD5, petroleum products (hydrocarbons), phenolandphenol derivatives, organochlorinepesticides, volatileorganohalogencompounds, heavymetals, surface-activeagents (surfactants),polycyclicaromatichydrocarbons (PAHs), etc. Atmosphericairof residential and sanitary protection zones: • Sample collection, meteorological parameters, formaldehyde, phenol, hydrogensulfide, PAHs, aliphaticandaromaticamines, nitrogenoxideandnitrogendioxide, methanol, methylmercaptan, sulfurdioxide, dust, gamma-emittingradionuclides,etc. Atmosphericairand the air of operational areas: • Ozone, nitrogenoxides, hydrogensulfide, sulfurdioxide, carbonmonoxide, petroleumhydrocarbons (C12-C19), hydrocarbons (methane), methane, methylmercaptan, ethylmercaptan, phenols, formaldehyde, synopticparametersand etc.

  6. SCOPE OF ACCREDITATION OF TL Soilsand bottom sediments: • Sample collection,Granulometriccomposition, pH (waterextract), carbonatesandbicarbonates, sulfates, chlorides, nitrates, calcium, potassium, sodium, magnesium, hydrogen sulfide, petroleum products (hydrocarbons), phenolandphenol derivatives, organochlorinepesticides, polychlorinatedbiphenyls, heavymetals, polycyclicaromatichydrocarbons (PAHs), gamma-emittingradionuclides, etc. Production facilities of enterprises (workplaces): • Noise, vibration, light, electric field, magnetic flux density, intensity of electromagnetic field of industrial frequency, intensity of electrostatic field.

  7. TESTING LABORATORY EQUIPMENT Basicequipment: • Gas chromatographs GC Agilent 7890 AMSD5975CandGC Agilent 7890 AECD and FID, Chromatec-Crystal 5000 • Liquidchromatograph (HPLC Agilent 1200), • AASwithhydride techniques and electrothermalatomisationproduced by Analytic Jena; • Microwave oven for soil and sediments samples preparationproduced by Analytic Jena; • Mass spectrometer with inductively coupled plasma (Agilent 7700x ICP-MS), • capillary electrophoresis instrument (Agilent 7100).

  8. TESTING LABORATORY EQUIPMENT • Analytical SieveShakerАS200 control (Retsch), • AutomaticTitrator 905 Titrando (Metrohm), • SpectrophotometerПЭ-5300-ВИ, • Spectrophotometers HACH-LANGE DR/2800 • Instrument for water-steam distillationUDK 129, • Fluid analyzerAnion 4100,etc. Auxiliaryequipment: Analytical and technical balances, ice baths, sand baths, ultrasound baths, magnetic stirrers with heater, thermostat, heating stoves, ovens, heating mantles, laboratory refrigerators, etc.

  9. STAFF • The laboratory employs 25 highly qualified specialists : leading chemical engineer, quality manager, HSE engineer, instrumentation and automation engineer, chemical engineers, chemists. • All the specialists have been trained at seminar «ST RK ISO/IEC 17025-2007 - General requirements for competence of testing and calibration laboratories» and «Features of accreditation of laboratories for ST RK ISO/IEC 17025-2007. Evaluation of measurement uncertainty». • All engineers, chemists and technicians have been trained at CIKV in Saint-Petersburg, Russia in methods of work using measuring instruments produced by «Agilent Technologies».

  10. Quality Control Sampling: • Quality of laboratory utensils cleanness (ISO compliance, all containers are preliminary decontaminated in laboratory, test report is submitted), multiple-use equipment is decontaminated; • Blind sampling program, rinseate samples, replicate samples, blank sample, blank transportationsample; • Calibration and adjustment of instruments with use of second source materials (before and after measurements); • Quality certificates issued by manufacturers of chemical reagents (highly purified material, reagent-grade, analytical reagent) used for equipment decontamination or sample preservation; • Strict observance of SOP of sampling and equipment decontamination (deactivation) between sampling points location;

  11. Quality Control Laboratory work : • Measuring instruments are registered in the RK Register and calibrated; • Quality Certificates issued by manufacturers of chemical reagents (highly purified material, reagent-grade, analytical reagent), used for testing; • Ready solvents expiration period shall not be longer than expiry period established by manufacturer; • Calibration and adjustment of instruments with use of second source materials; • Minimum number of initial calibration points is 5, linearity is determined by R2 factor; • During measurement process one point of calibration curve (median) is checked every 10 measurements (CCV); • In addition, blank sample (BLK) and laboratory control sample (LCS) are prepared.

  12. Participation in interlaboratory comparison tests and audit from Client Interlaboratory comparison tests: • April, 2014.LLP «Ecohydrocontrol» • June, 2014.Chemex Audits: • May, 2014. NCPOC • August, 2014. National Centre of Accreditation • September, 2014.NCPOC • September, 2014.TCO

  13. PROSPECTS FOR DEVELOPMENT • The expansion of Accreditation Scope of TL in Aktau • The creation of a testing laboratory in Atyrau • Accreditation of hydrobiological laboratory

  14. Laboratory Combined MRA Mark is a confirmation of the high quality of performed work

  15. LICENSE FOR PRECURSORS

  16. THANK YOU FOR ATTENTION!

More Related