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Echemi Chemical Products 4-Piperidineethanol Description

white crystalline low melting solid

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Echemi Chemical Products 4-Piperidineethanol Description

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  1. CAS No:622-26-4 Formula:C7H15NO Synonyms:4-Piperineethanol;4-PIPERIDINEETHANOL;4-ethanolpiperidine;piperidine-4-ethanol;PI PERIDIN-4-YLETHANOL;PIPERIDINEETHANOL(4-);2-Piperidin-4-ylethanol;4-Piperidineethanol,97%; 4-Piperidineethanol 97%;2-(4-Piperidinyl)ethanol China Export:From 2018.11 to 2019.11, total export volume of 4-Piperidineethanol from China was 99,860,829KG while total export value was $1,973,802,887. The biggest proportion of exporting volume in the last 12 months was 10.61% in 2019.05. Echemi Chemical Products 4-Piperidineethanol Description white crystalline low melting solid Echemi Chemical Products 4-Piperidineethanol Basic Attributes CAS No：622-26-4 Molecular Formula ：C7H15NO Molecular Mass ：129.2 Exact Mass ：129.115356 PSA ：32.3 A^2 LogP ：0.2 EINECS ：210-727-7 InChIKeys ：LDSQQXKSEFZAPE-UHFFFAOYSA-N H-bond Acceptor ：2 H-bond Donor ：2 SP3 ：1.00 RBN ：2 Echemi Chemical Products 4-Piperidineethanol Characteristics Density ：0.9±0.1 g/cm3 Melting Point ：46-47 °C(lit.) Bolling Point ：131-136 °C17 mm Hg(lit.)

  2. Flash Point ：>230 °F Refractive Index ：1.454 Echemi Chemical Products 4-Piperidineethanol Safety Information HS Code ：2933399090 UN No. ：NONH for all modes of transport WGK_Germany ：3 Risk Code ：36/37/38 Safety Instructions ：26-37/39-24/25 Dangerous Mark ：Xi P Code ：P261-P305 + P351 + P338 Hazard Statements ：H315-H319-H335 Hazard Note ：Irritant Echemi Chemical Products 4-Piperidineethanol Product Usage 4-Piperidineethanol have been used as a intermediate in the synthetic preparation of cellular-active allosteric inhibitors of FAK Echemi Chemical Products 4-Piperidineethanol Production Methods

  3. (0.06 mol) of lithium tetrahydride was added to anhydrous tetrahydrofuran (80 mL) under a nitrogen atmosphere under ice-cooling, and 4.95 g (0.03 mol) of pulverized 4-piperidine acetic acid was slowly added to the reaction solution , In which the reaction temperature was controlled to be less than 30 ° C. The reaction was allowed to proceed at 25 ° C overnight. The temperature was lowered to 0 ° C, and 3 mL of water, 3 mL of 30percent aqueous sodium hydroxide and 3 mL of water were gradually added dropwise. The mixture was stirred at 25 ° C for 30 min. The solvent was evaporated under reduced pressure to give 2.23 g (62.5percent) of a light yellow solid.

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