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Distillation is an ancient process which is believed to have been first experimented with in the Middle East as far back as 3000BC. It was most probable that what was produced was made from grapes or flowers rather than grain. Items like rice, About The first recoded distillation of a spirit in Scotland was recorded on a scroll where it was written “To Friar John Cor, by order of the King, to make aquavitae, VIII bolls of malt”. In this day 8 bolls of malt is enough to make around 1250 bottles of whisky so it was not a practise run but a previously sampled delicacy.