Oven with generator on the left middle vessels in the center
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11mm diameter. 33mm diameter. Oven with generator on the left middle (vessels in the center). 11mm diameter. 33mm diameter. E Field Distribution (Input Signal: 2.45GHz, 1 watt). 11mm. 33mm. Variation of E Field. 33mm diameter11mm diameter. Configuration of MARS.

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Oven with generator on the left middle (vessels in the center)

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Oven with generator on the left middle vessels in the center

11mm diameter

33mm diameter

Oven with generator on the left middle (vessels in the center)


E field distribution input signal 2 45ghz 1 watt

11mm diameter

33mm diameter

E Field Distribution(Input Signal: 2.45GHz, 1 watt)


Variation of e field

11mm

33mm

Variation of E Field


Configuration of mars

33mm diameter11mm diameter

Configuration of MARS


E field distribution in mars oven di water 25degc

E Field Distribution in MARS Oven (DI-Water 25degC)


Relationship of permittivity of di water with temperature

Relationship of Permittivity of DI-Water withTemperature


Permittivity of water vs temperature at 2 45ghz

Permittivity of Water VS Temperature (at 2.45GHz)


Measurements of the precursor solution at various temperature e

Measurements of the Precursor Solution at various Temperature (e’)


Measurements of the precursor solution at various temperature e1

Measurements of the Precursor Solution at various Temperature (e’’)


Extrapolation of permittivity of precursor solution at 175degc

e’

e’’

Extrapolation of permittivity of Precursor Solution at 175degC


Permittivity of the precursor and di water

Permittivity of the precursor and DI-water


E field distribution of mars 5 separate pictures

E Field Distribution of MARS-5(separate pictures)


Comparison of e field maxima

Comparison of E Field maxima


Discussion

Discussion

Given other same conditions

  • E field at middle plane of the reactor is higher than the bottom

  • E field for precursor is lower than water (due to higher loss tangent of precursor)

  • For water, temperature goes up -> loss tangent goes down -> E field goes up

  • For precursor, temperature goes up -> loss tangent goes up -> E field goes down

  • For MARS-5 oven, E field maxima for 33mm reactor is lower than 11mm reactor


Power with time of mars for silicalite synthesis

Power with time of MARS for silicalite synthesis


Maxima e field in mars for precursor solution normalized with sqrt power

Maxima E field in MARSfor precursor solutionNormalized with sqrt(power)


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