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Chemical Science and Technology Laboratory Overview

Chemical Science and Technology Laboratory Overview. James Whetstone, Chief Process Measurements Division. Process Analytical Technologies Subcommittee Meeting June 12 – 13, 2002 Rockville, MD. Chemical Science and Technology Laboratory. NIST … enabling a better future.

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Chemical Science and Technology Laboratory Overview

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  1. Chemical Science and Technology Laboratory Overview James Whetstone, Chief Process Measurements Division Process Analytical Technologies Subcommittee Meeting June 12 – 13, 2002 Rockville, MD Chemical Science and Technology Laboratory

  2. NIST … enabling a better future NIST Vision …is to be the global leader in measurement and enabling technology, delivering outstanding value to the nation. NIST Mission … is to develop and promote measurement, standards, and technology to enhance productivity, facilitate trade, and improve the quality of life. • Core Values: • People … we respect, value and support each other in all our activities. • Integrity … we are objective, ethical, and honest. • Customer focus…we anticipate the needs of our customers and are committed to meeting or exceeding their expectations. • Excellence… we expect world-class performance and continuous improvement in all we do.

  3. Electric Power Information & Semiconductor Technology Cell Phones …working with U.S. Industry Improving the Economy: Refrigerants Automobiles Improving the Quality of Life: Dentistry Mammography Smoke Detectors Medical Tests Cancer Treatment Body Armor

  4. DirectorArden Bement National Quality Program Harry Hertz Deputy DirectorKaren Brown TechnologyServices Manufacturing Extension Partnership Advanced Technology Program Director for Administration Jorge Urrutia Richard Kayser Marc Stanley (Act.) Kevin Carr ManufacturingEngineeringLaboratory PhysicsLaboratory Electronics andElectricalEngineeringLaboratory Materials Scienceand EngineeringLaboratory InformationTechnologyLaboratory Building and FireResearchLaboratory Chemical Scienceand TechnologyLaboratory Wm. Anderson Dale Hall Katharine Gebbie Leslie Smith Susan Zevin (Act.) Jack Snell Hratch Semerjian National Institute of Standards and Technology Boulder Laboratories Vacant

  5. DirectorArden Bement National Quality Program Harry Hertz Deputy DirectorKaren Brown TechnologyServices Manufacturing Extension Partnership Advanced Technology Program Director for Administration Jorge Urrutia Richard Kayser Marc Stanley (Act.) Kevin Carr National Institute of Standards and Technology Boulder Laboratories Vacant ManufacturingEngineeringLaboratory PhysicsLaboratory Electronics andElectricalEngineeringLaboratory Materials Scienceand EngineeringLaboratory InformationTechnologyLaboratory Building and FireResearchLaboratory Chemical Scienceand TechnologyLaboratory Wm. Anderson Dale Hall Katharine Gebbie Leslie Smith Susan Zevin (Act.) Jack Snell Hratch Semerjian

  6. CSTL Vision A world class research laboratory recognized by the Nation as the primary resourcefor chemical, biomolecular, and chemical engineering measurements, data, models, and reference standardsrequired to enhance U.S. industrial competitiveness in the world market. CSTL Mission • As the Nation’s Reference Laboratory, CSTL’s Mission is to provide the chemical measurement infrastructureto: • enhance U.S. industry's productivity and competitiveness; • assure equity in trade; and • improve public health, safety, and environmental quality.

  7. CSTL Goals • Measurement Standards • Establish CSTL as the pinnacle of the national traceability and international comparability structure for measurements in chemistry, chemical engineering and biotechnology, and provide the fundamental basis of the nation’s measurement system • Chemical and Process Information • Assure that U.S. industry has access to accurate and reliable data and predictive models to determine the chemical and physical properties of materials and processes • Measurement Science • Anticipate and address next generation measurement needs of the nation, by performing cutting-edge research

  8. CHEMICAL SCIENCE AND TECHNOLOGY LABORATORY Hratch G. Semerjian, Director William F. Koch, Deputy Director Biotechnology V. Vilker, Act. Chief Process Measurements J. Whetstone, Chief Surface & Microanalysis Science R. Cavanagh, Chief Physical & Chemical Properties M. Haynes, Chief Analytical Chemistry W. May, Chief • Experimental Kinetics & Thermodynamics • Chemical Reference Data & Modeling • Computational Chemistry • Experimental Properties of Fluids • Theory & Modeling of Fluids • Cryogenic Tech. • DNA Technologies • Bioprocess Engineering • Structural Biology • Biomolecular Materials • Fluid Flow • Fluid Science • Process Sensing • Thermometry • Pressure and Vacuum • Thermal and Reactive Processes • Atmospheric Chemistry • Microanalysis Research • Surface & Interface Research • Analytical Microscopy • Spectrochemical Methods • Organic Analytical Methods • Gas Metrology & Classical Methods • Molecular Spectroscopy & Microfluidic Methods • Nuclear Methods Organized by Discipline …

  9. CSTL Programs Microelectronics Transportation Biomaterials Energy Systems Environmental Technologies Nanotechnology Forensics Biotechnology Chemical and Allied Products Healthcare Food and Nutrition Data and Informatics Industrial and Analytical Instrument Services International Measurement Standards … Focused by Customer-Driven Programs

  10. ACSL NIST Boulder NIST Charleston CARB CSTL Facilities

  11. CSTL Activities Impacting Process Analytical & Process Measurements • Standard Reference Materials • Raman Spectroscopy – Intensity Standards • Spectrophotometry – Optical Absorbance Standards • Reference Data • NIR Spectral Data Directly Tied to U.S. National Gas Concentration Standards • Mass Spectrometric Database and Spectral Diagnostic Tools • Protein Data Bank – Biomolecular Structures • Instrument Calibration Services • Temperature, Pressure, Vacuum, Humidity, Flowrate, and Liquid Volume and Density

  12. nm 500 525 550 575 600 625 Broadband fluorescence from uranyl silicate glass Intensity Standards for Raman Spectroscopy Objective: Provide (first-ever) standard for intensity and frequency shift of Raman signals Customers: Instrument mfrs., chemical processing, DoD, DoE, pharmaceutical Industry Form: Uranyl Silicate Glass standard cuvette geometry • Status: • Evaluated prototype standard with ASTM Committee • First SRM (785 nm) by 9/2002 • Next Steps: Develop additional SRMs (488, 514.5, 533, 633, 1064 nm) Impacts: These standards will transform Raman from qualitative lab diagnostic into process instrumentation, allowing quantitative comparison of instrument response in differing locations and installations

  13. IFPAC 2003 – January 2003 An opportunity to interact with Process Analytical Specialists in a Range of Industrial Applications NIST Mission … is to develop and promote measurement, standards, and technology to enhance productivity, facilitate trade, and improve the quality of life. • Assist Industry and Other Government Agencies to improve measurements, measurement standards, technologies, and practices.

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