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1D-NMR lesson 1 module 1 Acquisition and treatment of NMR data Prof. Claudio Santi PowerPoint PPT Presentation


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1D-NMR lesson 1 module 1 Acquisition and treatment of NMR data Prof. Claudio Santi. Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia. 1D-NMR Introduction.

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1D-NMR lesson 1 module 1 Acquisition and treatment of NMR data Prof. Claudio Santi

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1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR lesson 1 module 1

Acquisition and treatment of NMR data

Prof. Claudio Santi

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Introduction

Mo represent a convenient way to describe a complete spin system. It is the vectorial sum of all the single vectors describing each single nuclear magnetic moment.

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Pulse NMR experimet

Pulse: Consist into applying a complete set of radio frequencies able to excite all the observed nuclei at the same time.

Mo during the pulse, moves from the equilibrium (z axis) describing a spiral.

After the pulse the system come back to the equilibrium giving rise the NMR signal

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

The rotating frame

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Free Induction Decay

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

FT-NMR treatment of the signal

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Digital Resolution

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (Shimming)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (RG)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (NS)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (LB)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (LB-GB)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (Phase)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (Phase)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Acqisition and Treatment (Phase Cycling)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR lesson 1 module 2

Decoupling techniques INEPT-DEPT

powerful tools in 1D-NMR

Prof. Claudio Santi

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Homo Decoupling

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Hetero Decoupling

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

BB Decoupling

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Off Resonance Decoupling

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Polarization Transfer

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Polarization Transfer

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Polarization Transfer

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling (INEPT)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling (refocused INEPT)

refocusing

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling (refocused INEPT-BB)

refocusing

INEPT

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling & INEPT

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Comparing different experiments

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Comparing different experiments

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling (DEPT)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling (DEPT)

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Decoupling

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

15N INEPT

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Taxol

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

Introduction

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

additional

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

pulse angle

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

additional quadrature detection

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


1d nmr lesson 1 module 1 acquisition and treatment of nmr data prof claudio santi

1D-NMR

additional

Prof. Claudio Santi Department of Chemistry and Technology of Drugs University of Perugia


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