1 / 7

Gravimetric Determination of Iron as Fe2O3

Purpose. To determine the amount of Iron (III) in a sample of unknown using the gravimetric analysis method. . Gravimetric Analysis?. Any analytical method that relies on measuring the mass of a substance to complete the analysis.. How to obtain the product?. PrecipitationTreating the analyte with a suitable counter ion (base).Dehydration/IgnitionHeated to drynessTo achieve a reproducible, stable composition.To change the chemical form of the precipitant..

Jimmy
Download Presentation

Gravimetric Determination of Iron as Fe2O3

An Image/Link below is provided (as is) to download presentation Download Policy: Content on the Website is provided to you AS IS for your information and personal use and may not be sold / licensed / shared on other websites without getting consent from its author. Content is provided to you AS IS for your information and personal use only. Download presentation by click this link. While downloading, if for some reason you are not able to download a presentation, the publisher may have deleted the file from their server. During download, if you can't get a presentation, the file might be deleted by the publisher.

E N D

Presentation Transcript


    1. Gravimetric Determination of Iron as Fe2O3 Experiment 3

    2. Purpose To determine the amount of Iron (III) in a sample of unknown using the gravimetric analysis method.

    3. Gravimetric Analysis? Any analytical method that relies on measuring the mass of a substance to complete the analysis.

    4. How to obtain the product? Precipitation Treating the analyte with a suitable counter ion (base). Dehydration/Ignition Heated to dryness To achieve a reproducible, stable composition. To change the chemical form of the precipitant.

    5. Precipitation Measures taken to reduce super saturation and form easily filtered particles (precipitate): High temperature during precipitation. Slowly adding and vigorously mixing the reagents. Maintaining a large sample volume. Using homogenous precipitation.

    6. Reaction! Formation of precipitate: Fe3+ + (2 + x)H2O (base)? FeOOH.xH2O(s) + 3H+ FeOOH.xH2O(s) (heat)? Fe2O3(s)

    7. Question? Why is the analyte treated with a counter ion?

    8. Answer To promote precipitation.

More Related